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Geophysical Imaging of Archaeological Materials at Iyekere, Ile-Ife Southwestern Nigeria

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Non-invasive geophysical methods are increasingly being used in archaeological studies. In this study, magnetic and electrical resistivity tomography geophysical techniques were integrated to locate subsurface archaeological materials. The survey consists of four parallel and three perpendicular profiles with station interval of 0.5 m for both magnetic and electrical resistivity tomography. Wenner array with electrode spacing ranging from 0.5 - 3.0 m was used to collect the electrical resistivity data. The results show that high total magnetic intensity anomalies correspond to high inverse model resistivities. The regions with high magnetic and resistivity anomalies were thought to be locations of archaeological materials; the corresponding depths to these materials were inferred from the resulting geophysical images. Test units conducted at the regions of high total magnetic intensity and inverse model resistivity yield archaeological materials including burnt pipes (Tuyere), iron slag, iron smelting, and pottery fragments at approximate depths inferred from the geophysical images.
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Journal of Environment and Earth Science www.iiste.org
ISSN 2224-3216 (Paper) ISSN 2225-0948 (Online)
Vol.5, No.2, 2015
148
Geophysical Imaging of Archaeological Materials at Iyekere, Ile-
Ife Southwestern Nigeria
K. D. Oyeyemi
1*
, M. A. Oladunjoye
2
, A. I. Olayinka
2
and A. P. Aizebeokhai
1
1. Department of Physics, College of Science and Technology, Covenant University, Nigeria
2.
Department of Geology, University of Ibadan, Nigeria
* E-mail of the corresponding author: kdoyeyemi@yahoo.com
Abstract
Non-invasive geophysical methods are increasingly being used in archaeological studies. In this study, magnetic
and electrical resistivity tomography geophysical techniques were integrated to locate subsurface archaeological
materials. The survey consists of four parallel and three perpendicular profiles with station interval of 0.5 m for
both magnetic and electrical resistivity tomography. Wenner array with electrode spacing ranging from 0.5 – 3.0
m was used to collect the electrical resistivity data. The results show that high total magnetic intensity anomalies
correspond to high inverse model resistivities. The regions with high magnetic and resistivity anomalies were
thought to be locations of archaeological materials; the corresponding depths to these materials were inferred
from the resulting geophysical images. Test units conducted at the regions of high total magnetic intensity and
inverse model resistivity yield archaeological materials including burnt pipes (Tuyere), iron slag, iron smelting,
and pottery fragments at approximate depths inferred from the geophysical images.
Keywords: Archaeogeophysics, Artefacts, ERT, Magnetic methods, 2D imaging
1. Introduction
Archaeological investigations and environmental impact assessments as part of development planning often
require geophysical surveys. The geophysical surveys are often designed to detect and define
archaeological structures and features that may be hidden beneath the subsurface. Environmental impact
assessments normally take place in advance of projects such as road or pipe corridors, the building of single
houses or estates and the development of industrial zones or mineral extraction sites. In the case of
archaeological research projects and monument delimiting surveys where there are known or visible
archaeological monuments, geophysical surveys can be used to assess their possible hidden sub-surface
extension and preservation, preservation potential or to prospect for undiscovered monuments in the
locality.
Geophysical methods provide fast, economical, efficient and non-destructive reconnaissance surveying
techniques often required by archaeologists. Also, geophysical techniques offer rapid, uniform,
reconnaissance for an entire site together with a synoptic view of the interrelationships within the site
(Weymouth and Huggings 1985). Geophysical methods has been used to map archaeological materials such
as healths, klins, buried bricks, building foundations, middens (trash heaps), burial tombs, ditches and soils
compacted or excavated by previous human activities (e.g. Weymouth 1986; Witten 2006; Cardarelli 2009;
Loperte
et al.
2011). In this study, high resolution geophysical methods involving magnetic method and
electrical resistivity tomography (ERT) have been used in the search for archaeological materials (iron slag
pottery materials, burnt pipes or Tuyere) in the investigation site. The locations and approximate depths to
these archaeological materials were inferred from the resulting geophysical images; pitting was carried out
at these locations to verify the accuracy of the geophysical results.
2. Study Area
Historical Background
The study area is located within Iyekere in Ile-Ife with an area 1575 square-metres (Figure 2). Iyekere is an iron
smelting archaeological site located near the disputed boundary between Ife and Modakeke communities in the
ancient city of Ile-Ife, southwestern Nigeria. It is boarded by latitudes 4
0
30 N and 4
0
33 N and longitudes 7
0
22 E
and 7
0
25 E (Figure 1). According to the oral tradition; Ile-Ife is regarded by all Yorubas as their immediate
ancestral origin where their ancestors dispersed to establish towns in their present homeland in West Africa. It is
considered to be the traditional birthplace of the Yoruba civilization, of the later part of the African Iron Age that
span between the second and the tenth centuries AD. Ile- Ife was a centre of the iron manufacturing, most
importantly of small wares, such as nails, horse-shoes, keys, locks, and common agricultural tools; and it was
estimated that there were about 500 iron smelters, smiths and other workers in iron of various kinds living within
a radius of about twenty kilometres (Adeniji 1977). Within the Yorubas, the knowledge of mining and metallurgy
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was prevalent among the royalty for iron mining and smelting majorly due to the need to acquire weapons to
fight and conquer more lands and empires (Ige and Rehren 2003).
Archaeological finds relating to iron smelting including black sand (slags) and iron stones have been recorded
within the study area by Ige and Rehren (2003). In their study, the chemical and mineralogical analysis revealed
the slags to be tapped with rich level of titanium oxide. A very high level of vanadium of around 2000 ppm V
2
O
5
was also reported. There are other archaeological sites in Ile-Ife that have been excavated by various researchers
amongst which are Ita Yemoo site (Willett 1970), Odo-Ogbe site (Eyo 1974), Woye Asiri and Obalara site
(Garlake 1977). The finds or archaeological deposits recovered from these sites were terracotta, bronze sculpture
and potsherd pavements which formed part of the materials ensembles of cultural efflorescence and elaborate
socio-political institutions in Ile-Ife between the 11
th
and 16
th
centuries (Eyo 1974).
Figure 1: Location map of Iyekere, Ile-Ife and its environs
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Figure 2: Survey base map showing profile lines and Pitting points.
Geological Setting
Geologically, the study area (Figure 3) is situated within the crystalline basement complex of Nigeria which
consist of early Proterozoic (2200 My) granite-gneiss, gneisses and schists (Oyawoye 1972). The schists consist
of mica-garnet bearing rocks intimately associated with mafic to ultramafic rocks. These rocks have been
extensively studied and characterized by several authors (e.g. Ige and Asubiojo 1991; Ige et al. 1998). The
greenstones which serve as the parent rocks for the lateritic ores occur as lenses within the polydeformed
migmatite gneiss complex. Several outcrops reportedly occur along the 800 km-long greenstone belt of Nigeria.
Their mineralogical composition consists mainly of iron-magnesium amphiboles and ore minerals such as spinel,
pyrrhotite, and pyrite. The area is located within the tropical rain forest with high temperature and high humidity.
Thick lateritic ironstones which are products of in situ weathering of some high Fe-Mg ultramafic rocks are
uniquely abundant within the area.
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Figure 3: Geological map of Ile-Ife and its environs (after NGSA, 2004)
3. Methodology
Magnetic Method
The magnetic survey is a passive geophysical technique which depends on the contrasts in a magnetic property
between the feature of interest and its surrounding environment (Schmidt 2007). The most significant magnetic
properties for archaeological investigation are magnetic susceptibility and magnetization. As most archaeological
materials contain magnetic substances, they possess magnetic properties that result to magnetic anomalies
observed in magnetic surveys which can be applied in different ways (Tarling 1983). Magnetometry is one of the
magnetic surveying methods which record the magnetic fields produced by a contrast in magnetization, whether
it is produced due to a magnetic susceptibility contrast, or remanent, for instance from thermoremanent
magnetization. In this study, the magnetic measurements were recorded using a proton magnetometer G-856AX
that involves measuring the total magnetic intensity component at each data point along the survey line. Seven
profiles involving four in-lines along NW-SE direction and three cross-lines (lines perpendicular to the in-lines)
were established (Figure 3). Station interval of 0.5 m was maintained across each profiles making a data density
of 770 points.
The magnetic sensor was oriented north during the survey, while the survey staff was maintained at 0.3 m above
the ground surface. The coordinates of the beginning and end points of each line were recorded by Geographic
Positioning System for applying in the Surfer software to create a plot of the survey area. A base station was set
up around 200.0 m away from the survey area which a G-856 magnetometer recorded magnetic readings at time
interval of one (1) minute in order to remove the diurnal variation effects of the earth’s magnetic field from
survey measurements. The magnetic data processing was carried out by inspecting raw data for spikes, gaps,
instrument noise or any other irregularities in the data. The next step involved diurnal variation correction and
International Geomagnetic Reference Field (IGRF) correction. Once the corrections were done, the data were
exported into a grid file to the program Surfer 8. After calculating a grid from XYZ data in Surfer, residual was
carried out to compute the difference between a grid value and the raw data at any XY location.
Electrical Resistivity Tomography (ERT) Method
Resistivity variations are generally known to correlate well with the lithological nature of the earth materials and
have been used as a tool in subsurface stratigraphic characterization (e.g. Aizebeokhai and Oyeyemi 2014), thus
providing important information in order to locate buried archaeological remains. The use of resistivity in
identification of walls has long been a common practice in archaeological investigations (Sarris and Jones 2000;
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Drahor et al. 2008; Tsokas et al. 2008; Tsokas et al. 2009; Berge and Drahor 2011). A total of seven multi-
electrodes 2D geoelectrical resistivity imaging lines were measured using the Wenner-alpha array. The length of
the 2D traverses ranges from a minimum of 30 m to a maximum of 75 m. The electrode spacing ranged from 0.5
to 3.0 m with an interval of 0.5 m. Line 2, 3, 5, and 6 were conducted the E-W direction whereas the other three
2D traverses (lines 1, 4, and 7) were conducted in the N-S direction (Figure 3).
RES2DINV computer code (Loke and Barker 1996) was used in the inversion of the 2D apparent resistivity data.
Nonlinear optimization technique which automatically determines 2D resistivity model of the subsurface for the
input apparent resistivity data (Griffiths and Barker 1993; Loke and Barker 1996) together with least square
inversion and smoothness constraints were applied.
Excavations
Three test units of 1.0 m x 1.0 m x 1.0 m were excavated within the archaeological site, Iyekere, Ile-Ife. Units 1
and 2 coincide with areas of high total magnetic intensity and high inverse model resistivity from the results of
magnetic method and the 2D resistivity tomography inversion modelling around the corresponding points of
intersection of Lines 3 and 7, and Lines 6 and 7 respectively. Unit 3 however lies along Line 4 coinciding with
the area of low total magnetic intensity and resistivity values. This serves as control (Figure 3) for the ground
thruthing process.
4. Results and Discussion
The 2D resistivity tomography inversion model sections of the E-W and N-S traverses which are perpendicular
to each other are presented alongside the total magnetic intensity profiles for proper integration to aid the general
interpretation (Figures 4 7). Along the total magnetic profile plot for each traverse, regions of magnetic high
correspond to those of high resistivity on the 2D tomography inversion model (Figures 6 and 7). The ERT result
of Line 1 (Figure 4) appears relatively noisy due to near surface resistivity variations. A major sharp drop in
magnetic signature was observed between 24.0 m and 40.0 m data points centring on 32.0 m point along Line 4
(Figure 5 ), which was about the lowest (-250 nT) in the entire study area. This is interpreted to be an evidence
of a backfilled ditch or well (Weymouth, 1986; Herwanger et al. 2000). The total magnetic intensity contour map
(Figure 4) and image map of the area (Figure 5) depicts region of very high magnetic intensity values to be
localized almost towards the centre of the study area. These high magnetic intensity areas are thought to be the
target areas for artefacts in archaeogeophysical studies (Mullins 1974; Weymouth 1986; Noel and Xu 1991;
Kvamme 2001; Hammerstedt et al. 2010) and can be inferred to be the points of intersection of both the E-W
Lines (lines 3 and 6) with the N-S Line 7 on the base map. These points coincide with the beginning of line 6
and within 25.0 m and 33.0 m data points on Line 3 as observed on 2D tomography inversion modelling results.
Figure 4: (a) Magnetic profiles and corresponding (b) 2D Electrical resistivity tomography imaging of Line 1
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Figure 5: (a) Magnetic profiles and corresponding and (b) 2D electrical resistivity tomography imaging of Line 4
Figure 6: (a) Magnetic profiles and corresponding and (b) 2D electrical resistivity tomography imaging of Line 5
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Figure 7: Magnetic profiles and corresponding 2-D electrical resistivity tomography imaging of Line 6
Fig. 8: Total magnetic intensity contour map showing test pits location
Legend
33200
Contour Map (nT)
Pit 2
Pit 1
Pit 3
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4.5536 4.5537 4.5538 4.5539 4.554 4.5541 4.5542 4.5543 4.5544 4.5545 4.5546
7.473
7.4731
7.4732
7.4733
7.4734
7.4735
7.4736
7.4737
7.4738
7.4739
32750
32800
32850
32900
32950
33000
33050
33100
33150
33200
33250
33300
33350
33400
33450
33500
33550
33600
33650
33700
33750
33800
33850
Figure 9: Total magnetic intensity colour image map showing the test pits location
The inventory of the findings from the excavated units (1 and 2) includes stone tools, Tuyere or burnt pipes, iron
smelting, broken pottery, some of which were found in their in-situ position while many were recovered (Figures
10 and 11). Also found within these units are rimsherd pottery, decorated potsherds, plane-sherd body pottery
and washed pottery. In Unit 2, a layer of charcoal was found in-situ (about 20 – 30 cm depth), iron slag, broken
pottery, Tuyere or burnt pipes and broken calabash were recovered (about 10 - 40 cm depth) beneath the top soil.
The charcoal within the study area was used for smelting and it was produced from special hard wood which are
distinguished by their poisonous characteristics (Ige and Rehren 2003). However, within Unit 3 which serves as
the control, sited along Line 4, no archaeological materials were recovered. The iron smelting and slags obtained
from the pitting were found to be similar to that reported by Ige and Rehren (2003).
Figure 10: Cultural materials from Unit 1: stone tools, Tuyère or bunt pipes ,iron smelting , iron slag ,pottery lids
and potsherds.
Pit 1
Pit 2
Pit 3
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Figure 11: Archaeological objects in their in situ position after removing the top soil (a), (b) and (c) Unit 1, (d),
(e) and (f) from Unit 2
5. Conclusions
The practical applications of geophysical techniques to delineate the locations and depths to archaeological
materials have been demonstrated. It was observed that regions of high magnetic intensity coincide with that of
high resistivity anomalies in most cases. Corroborative evidence from trial pitting shows that units located within
these regions yielded high quantities of cultural materials, while that located at low magnetic intensity and
resistivity anomaly was almost sterile of any archaeological deposit. Thus the study confirmed that geophysical
techniques are non- destructive, and provide the capability to map and analyse subsurface archaeological
materials and has been further proven to be an effective tool to expedite cultural preservation other than random
pitting.
Acknowledgements
We would like to thank the curator National Museum and Monuments Ile-Ife for permission to carry out this
research. The assistance of the Director of the Institute of African Studies, Obafemi Awolowo University Ile-Ife,
Nigeria, Dr.Ogunfolakan to facilitate this research is highly appreciated. Thanks also to the curator, Department
of Archaeology and Anthropology, University of Ibadan, Nigeria, Dr. Ajekigbe for his expertise during the
excavation.
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... The field survey revealed areas of iron slag deposits with characteristic black soils and fragments of tuyeres in addition to a suspected ancient waste discharge channel. These artefacts and features are typical of an iron smelting site (Friede 1979;Ige & Rehren 2003;Holl 2009;Oyeyemi et al. 2015). Adeniji (1977) claimed that about 500 iron smelters, smiths and workers of iron of various kinds lived within a radius of about 20 km in Ile-Ife (Fig. 1). ...
... Adeniji (1977) claimed that about 500 iron smelters, smiths and workers of iron of various kinds lived within a radius of about 20 km in Ile-Ife (Fig. 1). Other ancient iron smelting sites that had been identified and studied in the ancient city are in Iyekere, Akartabata and recently within the estate of Obafemi Awolowo University ( Fig. 1; Ige & Rehren 2003;Oyeyemi et al. 2015;Olorunfemi et al. 2021). At the time of the reconnaissance survey, the site was at risk of being destroyed. ...
... The magnetic low falls significantly within the zone where black soil/slag was observed and also at the southern edge of the study area while magnetic highs are observed in the northern half of the study area with peak amplitudes beneath the location where a tuyère fragment (feature 2 in Fig. 2) was found. Both maps (Fig. 4a, b) identify one major anomalous zone A (A 1 &A 2 ) that contains contiguous closures of magnetic low (negative), A 1 , and magnetic high (positive), A 2 , which are typical of a circular/oval-shaped furnace and an iron slag deposit respectively (Powell et al. 2002;Oyeyemi et al. 2015). The identified channel (feature 3 in Fig. 2) has no distinct magnetic signature and could just be a mere geomorphological feature. ...
... Geophysics has found useful applications as a reconnaissance tool in archaeological prospection (Eluyemi et al. 2012;Olorunfemi et al. 2015;Oyeyemi et al. 2015;Mohamed 2017). It is commonly used for the identification of prospective sites for excavation and estimation of archaeologically significant depth. ...
... In archaeological prospection, the magnetic and the electrical resistivity methods are commonly used (Drabor et al. 2008;Karaval et al. 2012;Caggiani et al. 2012;Eluyemi et al. 2012;Ekinci et al. 2014;Shaaban et al. 2014;Olorunfemi et al. 2015;Oyeyemi et al. 2015;Eyub 2017). The electromagnetic, Ground Penetrating Radar (GPR), Gravity and Seismic methods are also used (Carson 1962;Witten 2006;Batayneh 2011;Delan 2012;St Pierra et al. 2019). ...
... During a recent regional hydrogeophysical investigation for groundwater development, the field crew encountered iron slags, pieces of tuyeres, fragments of fired clay furnace wall and iron nodules that are scattered within a 70 m x 72 m piece of land within the estate of the Obafemi Awolowo University (OAU) in Ile-Ife, Southwestern Nigeria. These features are characteristics of an ancient iron smelting site (Friede 1979;Ige & Rehren 2003;Holl 2009;Eluyemi et al. 2012 andOyeyemi et al. 2015). The suspected OAU iron smelting site is the focus of an integrated geophysical investigation whose results are reported in this paper. ...
Chapter
Full-text available
Magnetic and resistivity surveys were carried out at an ancient iron smelting site located within the estate of the Obafemi Awolowo University (OAU), Ile-Ife, Southwestern Nigeria, with a view to identifying location(s) of its furnace(s) and other archaeological features and establishing the furnace structure and iron smelting history. Ground magnetic profiling, 1D Vertical Electrical Sounding (VES) and crossed (orthogonal) 2D Dipole-Dipole profiling techniques were adopted. The locations of four suspected iron smelting furnaces were identified based on oval-shape peak negative magnetic low closures, while the resistivity anomalies were mixed-low to moderately high, probably due to the nature of the furnace infill. Three suspected slag trenches were delineated based on peak positive magnetic highs with generally high resistivity anomalies. Two suspected ancient structure foundations were delineated based on rectangular-shape positive magnetic closure and similarly shaped high resistivity anomaly respectively. Two other suspected dug wells characterised by circular low resistivity closures were also identified. Based on literature review, field observations and geophysical characteristics, eleven sites were recommended for follow-up archaeological excavation. While it might be too early speculating on the likely raw materials used at the OAU iron smelting site, there were evidences of slags with imprints of fired grey gneiss foliation planes and partly burnt laterite.
... Urban infrastructural development has obliterated many of the sites and destroyed its archaeological features. One of the prominent iron smelting site is located in the premises of Anglican Secondary Commercial Grammar School, Iyekere, Ile-Ife (Figure 4), where an earth road and construction works within the school have exposed one rectangularshaped furnace site and relics of what looks like other sites with features typical of furnaces such as tuyere, fragments of clay furnace wall, iron slags, black soil residue (ash) and pottery fragments ( Figure 5(a-c); Oyeyemi et al. 2015). It is very rare to find exposed iron smelting furnace, which makes the site suitable for the preliminary study of the thermally induced enhanced resistivity effect of furnacing. ...
Article
Full-text available
We utilised resisto-thermal effect of iron smelting to precisely locate concealed furnaces and slag trenches at an ancient iron smelting site situated within the estate of Obafemi Awolowo University, Ile-Ife, Southwest Nigeria. The methodology involved closely spaced, small electrode spacing (micro) Vertical Electrical Soundings across diagnostic dipolar magnetic anomaly closures. Both the furnace and the slag trench sites were characterised by thermal induced enhanced layer resistivity values and anomalously high depth extent of an index (second) resisto-archaeological geoelectric layer with higher influence beneath the furnace than the slag trench. The results showed that the location of the furnace is shifted from the centre of the magnetic low (negative), sometimes overlapping the transition zone towards the magnetic high (positive) while the slag trench is generally situated within the magnetic high zone. Preliminary archaeological excavation at one of the investigated sites (site 1) identified a furnace and the adjoining slag trench structures at the precise locations predicted from the geoelectric section. The study concluded that thermal-induced resistivity attribute is effective in precisely locating concealed ancient iron smelting furnace and slag trench structures.
... Performing geophysical prospecting prior to archaeological excavations is not yet a widespread approach in Sub-Saharan field archaeology, although the number of projects using geophysical methods has noticeably increased in this century (e.g. Magnavita and Schleifer 2004;Gaffney et al. 2005;Pollard and Banks 2005;Magnavita et al. 2006Magnavita et al. , 2007Magnavita et al. , 2009Fleisher et al. 2012;Neukirch et al. 2012;Wynne-Jones 2012;Ogah et al. 2014;Welham et al. 2014;Oyeyemi et al. 2015; for an overview see Magnavita 2016). The application of integrated geophysical prospecting on burial mounds in Sub-Saharan Africa is, however, truly novel. ...
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