Ahsltrom R&D
Question
Asked 5th Sep, 2022
How to acid digest waste-water sample before heavy metal analysis by ICP?
How to acid digest waste-water samples before heavy metal analysis by ICP? I need the protocol. Thanks
All Answers (3)
May vary depending on the target elements but you can try : 50 ml water + 3ml HNO3 (conc) + 2ml HCl (conc) ; will stabilize most elements.
Temperature, time and steps will depend on your equipment and its pressure capability ; normally, no need to go very high in temperature.
1 Recommendation
University of Central Punjab Lahore-Pakistan
A representative 45-milliliter (mL) aqueous sample is digested in 5 mL of concentrated nitric acid (HNO ) in a Teflon® digestion vessel using microwave heating. After the digestion process, the sample is cooled, and then filtered or allowed to settle in a clean sample bottle prior to analysis.
A representative 1 to 2 gram (wet weight) sample is digested with repeated additions of nitric acid (HNO ) and hydrogen peroxide (H O ). Hydrochloric acid (HCl) is added to the digestate and the sample is refluxed. The
digestate is then diluted to a final volume of 100 milliliters (mL) with deionized (DI) water.
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