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Transverse weld macrograph highlighting the various weld region: fusion zone (FZ), fine grain heat affected zone (FG-HAZ), coarse grain heat affected zone (CG-HAZ), base metal (BM), and location of Vickers hardness indentations.

Transverse weld macrograph highlighting the various weld region: fusion zone (FZ), fine grain heat affected zone (FG-HAZ), coarse grain heat affected zone (CG-HAZ), base metal (BM), and location of Vickers hardness indentations.

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Article
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The role of micro-alloying in the submerged arc welding (SAW) of high strength low alloy steel linepipe is paramount in facilitating the high strength properties of the linepipe. In this study, transmission electron microscopy analysis revealed the presence of large (0.85 µm) Ti (C,N) precipitates within the predominantly acicular ferrite SAW joint...

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... software package. A FIB microscope (FEI FIB200) and a dual-column FIB (Carl Zeiss Nvision N40) were used to prepare TEM specimens. The TEM specimen preparation methodology for steel samples has been documented in [20,21]. Cross weld Vickers hardness tests were made at 1 mm intervals across the OD weld, transverse to the SAW joint, as depicted in Fig. 1 using a 10 kg load with a 10 s loading time. Cross-weld Charpy V-notch (CVN) samples (50 mm  10 mm  10 mm, with 2 mm notch depth and 0.25 mm root radius) were produced and tested at 0 1C in accordance with API standard [18], the details of which including the location and orientation of the CVN samples with respect to the weld joint ...
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... . 1 shows the macrograph of the SAW seam weld of the UOE linepipe section used for the current investigation. When welding materials of a similar composition, epitaxial growth rather than nucleation occurs [22]. The solidifying grains grow anisotropically towards the heat flow resulting in the coarse and columnar FZ grain structure as ...
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... . 1 shows the macrograph of the SAW seam weld of the UOE linepipe section used for the current investigation. When welding materials of a similar composition, epitaxial growth rather than nucleation occurs [22]. The solidifying grains grow anisotropically towards the heat flow resulting in the coarse and columnar FZ grain structure as depicted in Fig. 1(a). Fig. 1(b) also highlights the various weld regions under examination across the SAW joint. It is clear from the image that the combined heat input of the two pass SAW has produced a defect free, fully penetrated weld, with a good weld bead shape. The high heat input from the SAW also created a visible HAZ of between 2 and 4 mm in ...
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... macrograph of the SAW seam weld of the UOE linepipe section used for the current investigation. When welding materials of a similar composition, epitaxial growth rather than nucleation occurs [22]. The solidifying grains grow anisotropically towards the heat flow resulting in the coarse and columnar FZ grain structure as depicted in Fig. 1(a). Fig. 1(b) also highlights the various weld regions under examination across the SAW joint. It is clear from the image that the combined heat input of the two pass SAW has produced a defect free, fully penetrated weld, with a good weld bead shape. The high heat input from the SAW also created a visible HAZ of between 2 and 4 mm in width at either ...
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... Δσ p is increment of yield strength in MPa, G is shear modulus (81,600 MPa), b is Burger's vector in mm (0.248 nm), D p is the average diameter of precipitates (0.85 mm) in mm, and f p is the volume fraction (0.103) of precipitates. Fig. 10 shows the increment of yield strength contribution for a range of precipitate sizes and volume fractions. For the SAW joint with a 0.103 volume fraction and 0.85 mm average diameter Ti (C,N) precipitates, a strengthening contribution of around 32.1 MPa is achieved. Fig. 10 also indicates that significant increase in weld metal strength ...
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... (0.85 mm) in mm, and f p is the volume fraction (0.103) of precipitates. Fig. 10 shows the increment of yield strength contribution for a range of precipitate sizes and volume fractions. For the SAW joint with a 0.103 volume fraction and 0.85 mm average diameter Ti (C,N) precipitates, a strengthening contribution of around 32.1 MPa is achieved. Fig. 10 also indicates that significant increase in weld metal strength could be achieved if the average precipitate size is below 0.5 mm due to the exponential nature of the curve. By plotting at 720% of the measured 0.103 volume fraction, it is also clear that an increase in the volume fraction of precipitates could also increase yield ...
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... the mean D p (0.85 mm) and d p (5.67 mm) values calculated from microstructural observations in our study, it is possible to assess the effect of mean size and spacing of precipitates on plane- strain fracture toughness. The results in Fig. 12 show a fracture toughness value of 36.6 MPa m 1/2 using the input data presented. This offers a conservative estimate around 11% below the fracture toughness values determined experimentally in Table 2. The low deviation and conservative nature of the prediction validates the integrity of the model presented. The stress triaxiality ...
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... fracture toughness values determined experimentally in Table 2. The low deviation and conservative nature of the prediction validates the integrity of the model presented. The stress triaxiality values predicted using Eqs. 3 and 4 give slightly low values ( $1.5) but offer good fracture toughness estimates in the case of this study. As shown in Fig. 12, fracture initiation toughness increases as the size of precipitates become smaller. The drop in fracture toughness as a result of coarsening is attributed to the reduced local ductility around the precipitate as a direct result of growth. Once nucleated, the cracks develop into spherical and ellipsoidal holes by plastic deformation, ...
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... perspective, an optimum combination of toughness and strength can be achieved by controlling the size of Ti (C,N) precipitates to less than 0.5 mm in the SAW weld X65 linepipes. However, if the volume fraction of particles is kept the same, reducing the precipitate size will cause the spacing of the precipitates to also reduce, as demonstrated in Fig. 13. This will lead to a reduction in fracture toughness according to Eq.(8). So, in order to be certain that K ic could be increased, while reducing mean precipitate size, the volume fraction of particles also needs to be reduced in order to increase the particle spacing or to at least to maintain its same level. But a reduction in the ...
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... Eq.(8). So, in order to be certain that K ic could be increased, while reducing mean precipitate size, the volume fraction of particles also needs to be reduced in order to increase the particle spacing or to at least to maintain its same level. But a reduction in the volume fraction of particles will cause yield strength to drop, as presented in Fig. 10. This is the classical scenario that an increase in yield strength of the steel will have to be compromised by a reduction in toughness, which is adequately demonstrated through the mathematical equations presented in the paper. Therefore these equations could be used the guide the design or selection of the steel chemistries for the ...

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... Moreover, diversity in the microstructure of the weld metal was inevitable because the proportion and size of the microstructure are easily influenced by welding process parameters and differences in the chemical composition of the filler metal. In the multi-pass weld metal, different heat inputs and cooling rates [23] generally influence the proportions of the columnar grain zone and reheated regions [24] and the characteristics of the transformation products, such as grain size, impurity or precipitate coarsening of alloying elements [25], then further affect the tensile strength and impact toughness. Furthermore, the welding speed, inter-pass temperature, and post-weld heat treatment (PWHT) can affect the properties of weld metals, particularly the impact toughness. ...
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