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Major element geochemical classification plots for granitoid rocks from Bétaré Oya. (a) Na2O + K2O versus SiO2 diagram of [35], showing the subalkaline compositions of the rocks. (b) K2O versus SiO2 diagram of [37], the rocks plot in the high-K field. (c) A/NK versus A/CNK diagram of [38] showing aluminosity and alkalinity. (d) Discrimination diagram of [39], showing that the rocks were formed in a volcanic arc setting. A/NK = molar Al2O3/Na2O+K2O; A/CNK= molar Al2O3/CaO+Na2O+K2O, Syn-COLG, Syn-collisional granitoid; WPG, within-plate granitoid; VAG, volcanic arc granitoid; ORG, oceanic ridge granitoid 

Major element geochemical classification plots for granitoid rocks from Bétaré Oya. (a) Na2O + K2O versus SiO2 diagram of [35], showing the subalkaline compositions of the rocks. (b) K2O versus SiO2 diagram of [37], the rocks plot in the high-K field. (c) A/NK versus A/CNK diagram of [38] showing aluminosity and alkalinity. (d) Discrimination diagram of [39], showing that the rocks were formed in a volcanic arc setting. A/NK = molar Al2O3/Na2O+K2O; A/CNK= molar Al2O3/CaO+Na2O+K2O, Syn-COLG, Syn-collisional granitoid; WPG, within-plate granitoid; VAG, volcanic arc granitoid; ORG, oceanic ridge granitoid 

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A combination of whole rock geochemistry, Ti-in-zircon thermometry, geochronology and Lu-Hf isotope composition of zircon is employed in this study to depict the source of a granitoid from the Bétaré Oya Gold District, its formation temperature, age of emplacement and evaluate the role of petrogenesis and magmatic evolution of the granitic melt in...

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... whole rock geochemical data for the studied granitoid samples alongside the Batouri granitoid [7] and the two mica granite [16] from Ekomédion are represented in Table 1 [35,36,37], the Bétaré Oya granitoid is sub-alkaline with a high-K calc- alkaline affinity (Figure 2a, Figure 2b). On the A/NK versus A/CNK classification plot [38], the granitoid is granodioritic to tonalitic in composition. ...
Context 2
... the A/NK versus A/CNK classification plot [38], the granitoid is granodioritic to tonalitic in composition. They are peraluminous with all samples clustering within the 'I- type' field ( Figure 2c). Nb -Y discrimination plot [39], reveals a volcanic arc setting for that the Bétaré Oya granitoid (Figure 2d). ...
Context 3
... are peraluminous with all samples clustering within the 'I- type' field ( Figure 2c). Nb -Y discrimination plot [39], reveals a volcanic arc setting for that the Bétaré Oya granitoid (Figure 2d). ...

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... Consequently, lithologic units within the domain bear pre-tectonic, syn-tectonic and posttectonic imprints. These are largely high-K, calc-alkaline rocks [9,10,30,31] interspersed with low-to medium-grade metamorphic rocks of volcano-sedimentary protoliths [32][33][34]. ...
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... 620 Ma, using LA-ICP-MS U-Pb zircon dating, whereas Lemdjou et al. (2022) argued for a single magmatic pulse based on indistinguishable LA-ICP-MS zircon U-Pb ages of 641 ± 3 Ma and 638 ± 4 Ma for the Doumba Bello and Ngoura granitic plutons, respectively. In the Batouri area, located south of Colomines, auriferous monzogranite and granodiorite were dated using U-Pb and Ar-Ar geochronology at ca. 619 and 624 Ma and 640-620 Ma, respectively (Asaah et al., 2015;Ateh et al., 2017). The variety of proposed emplacement ages for intrusions in the region demonstrates a continuing need to refine the timing of magmatism and its temporal links with associated gold mineralization throughout Eastern Cameroon and the central domain of the PANEFB in a broader context. ...
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... The association of the residual fraction with Pb is linked to formation of stable complexes [49]. Besides, high content of Pb in the residual fraction of tailings samples may be due to the presence of PbS (galena), the main form of an insoluble Pb occurring naturally in the study area [10,50]. This residual fraction of Pb is not available for plant uptake because it is associated with soil matrix and crystalline structure. ...
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... The orogenic assemblage of Cameroon consists of three major geotectonic units ( Fig. 1): (i) Archean-Paleoproterozoic basement gneiss, migmatite and granulite with available ages ranging from ca. 3.09 to 2.49 Ga (e.g., Caen-Vachette 1988;Van Schmus et al. 2008;Chombong and Suh 2013;Chombong et al. 2017), (ii) Meso-to Neoproterozoic volcano-sedimentary sequences that were deformed and metamorphosed to various degrees and yield zircon detrital U-Pb ages from ~ 1100 to 950 Ma , and (iii) Pan-African granitic rocks that intruded the (i-ii) units at ~ 680-520 Ma (e.g., Asaah et al. 2015;Ateh et al. 2017;Li et al. 2017;Embui et al. 2020) (Fig. 1). ...
... This is an important research theme in the Neoproterozoic fold belt north of the Congo Craton, considering that granitic plutonism is ubiquitous throughout the various stages of the orogeny from subduction, collision to crustal thinning. In the neighbouring Batouri and Bétaré Oya gold districts (Fig. 2b) of eastern Cameroon, the granitoids were constrained to an age bracket of 635-620 Ma (zircon U-Pb dating) and this age bracket has been tentatively linked to magmatic activity associated to gold mineralisation (Asaah et al., 2014;Ateh et al., 2017). These ages need further scrutiny and form the basis of this contribution with a focus on the Colomine auriferous granitoids, which are poorly known in terms of the ages and crustal contribution to their petrogenesis. ...
... In this paper, we present new zircon U-Pb ages and Lu-Hf isotope data from preto syn-collisional granites of the Colomine gold district. We use these data in combination with previously published Lu-Hf zircon data from Bétaré Oya granitoids (Ateh et al., 2017) to place additional constraints on the timing of gold-associated Colomine granites, and the relative importance of basement sources (mantle/crustal) in the generation of the Neoproterozoic continental crust in SE Cameroon. ...
... This suggests that the magmas from which the zircons crystallised contained a significant contribution of old crustal material of Archean to Paleoproterozoic age (Fig. 6b). The zircon Hf isotopic signatures from this study are clearly distinct from those of the Bétaré Oya granitoids (ϵHf (t) ; − 18.9 to +0.3, Fig. 6) located about 100 km farther north (Ateh et al., 2017), indicating different source reservoirs. Colomine zircons show variations up to 9 ϵHf (t) units, excluding one outlier zircon grain BC08-05 with up to about 20 ϵHf (t) units difference. ...
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The Neoproterozoic Pan-African Orogeny in the Adamawa-Yad´ e domain (AYD) of Cameroon is characterized by intense magmatism of metaluminous to weakly peraluminous I-type granites spatially associated with transcurrent shear zones. This domain provides a critical geological record that is important for unravelling the regional tectonic evolution and geodynamic setting. We present new zircon U-Pb ages and Lu-Hf isotope data from pre-collisional biotite granite and porphyritic K-feldspar granite of the gold-producing Colomine district. Zircon U-Pb ages of biotite granite samples suggest emplacement at 727 ± 8 Ma and at 671 ± 6 for the porphyritic K-feldspar granite. Metamorphic-hydrothermal events between 600 and 550 Ma resulted in Pb-loss of most dated zircons. Lu-Hf isotope data of zircon grains form the porphyritic K-feldspar granite with ϵHf(t) values of − 28.7 to − 22.6 and Tc DM ages of 2.4–2.1 Ga overlap with those of the biotite granite (ϵHf(t) values of − 29.4 to − 19.6; Tc DM ages of 2.5–1.9 Ga). Depleted mantle model ages and ϵHf(t) values suggest that the granites were derived from crustal reworking of older Archean to Paleoproterozoic crust with minor mixing from a juvenile component during the Pan-African. The formation of these pre-collisional granites is interpreted as related to accretion tectonics that started around 750 Ma and incorporating tectonic domains of the Central African Fold belt, namely, the NW Cameroon domain, Mayo-Kebbi domain and the Adamawa-Yade domain.
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... Moreover, the previous studies are controversial regarding the timing of sediment deposition and granitoid emplacement along the Lom Belt, as well as, of the primary gold mineralization. Toteu et al. (2006a) interpreted the sediments of the Lom Belt as being deposited, deformed, and metamorphosed within the period of 613-600 Ma, while granitic intrusion within the belt was dated at ca. 635 Ma (Ateh et al., 2017). Furthermore, plutonic rocks ages of 635 Ma (Bétaré Oya district) and 620 Ma (Batouri district) were equated to the age of gold mineralization (Asaah et al., 2015;Ateh et al., 2017), but mineralized veins cut both metavolcanic-metasedimentary and plutonic rocks (Azeuda Ndonfack et al., 2021a,b). ...
... Toteu et al. (2006a) interpreted the sediments of the Lom Belt as being deposited, deformed, and metamorphosed within the period of 613-600 Ma, while granitic intrusion within the belt was dated at ca. 635 Ma (Ateh et al., 2017). Furthermore, plutonic rocks ages of 635 Ma (Bétaré Oya district) and 620 Ma (Batouri district) were equated to the age of gold mineralization (Asaah et al., 2015;Ateh et al., 2017), but mineralized veins cut both metavolcanic-metasedimentary and plutonic rocks (Azeuda Ndonfack et al., 2021a,b). These inconsistencies result in a poor understanding of the chronology of events such as sediment deposition, plutonic rock emplacement, and gold mineralization in eastern Cameroon. ...
Article
The Bétaré Oya and Woumbou-Colomine-Kette gold districts, located in the East Metallogenic Province of Cameroon, are characterized by a complex Neoproterozoic history of metamorphism, polyphase deformation, and widespread crustal anatexis and magmatism. Controversy exists on the timing of the metamorphic and magmatic events, particularly within the area of the Lom Belt, and accurate absolute ages and even geodynamic chronology pertaining to the tectono-magmatism are yet to be well constrained. New LA-ICP-MS U-Pb zircon ages, Lu-Hf isotope data, and whole-rock geochemistry of granitoids and metavolcanic-metasedimentary rocks from the Woumbou-Colomine-Kette and Bétaré Oya districts better constrain the tectonic evolution of eastern Cameroon. The U-Pb age data of 646.5 ± 2.0 Ma, 643.7 ± 1.8 Ma, 641.3 ± 4.4 Ma, 641.4 ± 3.5 Ma, and 620.9 ± 2.6 Ma revealed that the granitoids from the Woumbou-Colomine-Kette district were emplaced during two main magmatic events at ca. 650-635 Ma and ca. 620 Ma. The zircon Hf(t) values between − 13.80 and − 6.20 with Hf TDM model ages of 1.9-2.4 Ga, coupled with geochemical signatures show that granitoids were generated by partial melting of Paleoproterozoic supracrustal metasedimentary units and meta-igneous rocks during subduction and orogenic convergence. Metamorphic zircons from the actinolite-chlorite schist of the Lom Belt gave ages between ca. 655 and 585 Ma, implying that the metavolcanic-metasedimentary rocks of the belt were deposited prior to 655 Ma, then metamorphosed and deformed between ca. 655 and 585 Ma. Two age peaks of detrital zircons were measured at ca. 1035 Ma and ca. 784 Ma with the εHf (t) values of-14.60 and-18.37 and +2.97 and +8.60, respectively. These data, coupled with those from previous studies, suggest that the Lom Belt may represent a suture zone between the Central and Southern Cameroon domains with an early rifting at ca. 784 Ma. In general, our U-Pb ages indicate compressional to transpressional deformational phases in the two districts at ca. 660-635 Ma (D1), 630-610 Ma (D2), and 600-580 Ma (D3). The latter D3 transpressional event was also associated with the formation of the widespread occurrences of orogenic gold, although the precise timing of gold deposition needs to be constrained.
... Plutonic rocks in the district are syn-tectonic (see below section 3.2) and show heterogeneous deformation features varying from undeformed to strongly deformed mineral grains within a single pluton (Ngako et al., 2003). The Bétaré Oya peraluminous, calc-alkaline granitic stock was emplaced into the chlorite-sericite schist and has a granodioritic to tonalitic affinity (Ateh et al., 2017). The pluton shows evidence of D2 sinistral deformation along its NW and NE margins when examined by aeromagnetic and radiometric images (Ateh et al., 2017), but the total amount of displacement along the Bétaré Oya Shear Zone is unknown. ...
... The Bétaré Oya peraluminous, calc-alkaline granitic stock was emplaced into the chlorite-sericite schist and has a granodioritic to tonalitic affinity (Ateh et al., 2017). The pluton shows evidence of D2 sinistral deformation along its NW and NE margins when examined by aeromagnetic and radiometric images (Ateh et al., 2017), but the total amount of displacement along the Bétaré Oya Shear Zone is unknown. The intrusion was dated at ca. 635 Ma and formed in a subduction-related magmatic arc setting (Ateh et al., 2017). ...
... The pluton shows evidence of D2 sinistral deformation along its NW and NE margins when examined by aeromagnetic and radiometric images (Ateh et al., 2017), but the total amount of displacement along the Bétaré Oya Shear Zone is unknown. The intrusion was dated at ca. 635 Ma and formed in a subduction-related magmatic arc setting (Ateh et al., 2017). Mafic dikes occur in the belt (Fig. 3e, 3i) and underwent the same regional greenschist facies metamorphism. ...
Article
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The Bétaré Oya district has a substrate composed of the Neoproterozoic metavolcanic-metasedimentary rocks of the Lom Belt in eastern Cameroon. The district is well-known for alluvial gold mining activities, however, the primary gold mineralization has received little attention. In the current study, we newly report geological, ore mineralogy, fluid inclusion microthermometric, laser Raman spectroscopy, and stable isotope data from auriferous veins of the Lom Belt to characterize the style of gold mineralization and to constrain the origin of the ore-forming fluids. The auriferous quartz veins are laminated, fractured, N- to NE-trending, and spatially associated with the Bétaré Oya Shear Zone. Fieldwork coupled with microscopic examination and the textural relationships of ore minerals revealed two stages of mineralization. The first stage is characterized by the presence of pyrite, sphalerite, galena, chalcopyrite, pyrrhotite, hematite, petzite, hessite, wolframite, electrum, and gold, while the second stage is characterized by the presence of a later deposition of galena and pyrite, as well as minor greenockite. The gangue minerals are quartz, sericite, muscovite, chlorite, calcite, ankerite, and barite, whereas the supergene assemblage (stage 3) includes goethite, hematite, covellite, and enargite. Two fluid inclusion assemblages containing three types of inclusions are identified in mineralized quartz veins. Assemblage 1 consists of gold-related types 1 and 2 with daughter minerals consisting of nahcolite, magnesite, and arsenolamprite (black native arsenic), whereas assemblage 2 consists of post-gold type 3 fluid inclusions. Type 1 has H2O-NaCl-CO2±N2±CH4 primary fluid inclusions (FI), with a TmCO2 ranging from −59.8 to −56.6 °C, salinities from 0.5 to 10.8 wt% NaCl eq., densities from 0.87 to 1.00 g.cm⁻³, and total homogenization temperatures between 280 and 360 °C. Type 2 contains CO2 (±H2O-NaCl)±N2±CH4 FI that exhibit TmCO2 ranging between −60.0 and −56.7 °C, ThCO2 from 13 to 25 °C, and densities between 0.73 and 0.85 g.cm⁻³. Type 3 shows H2O-NaCl FI with salinities between 0.2 and 10.1 wt% NaCl eq., densities between 0.82 and 0.98 g.cm⁻³, and total homogenization temperatures from 160 to 235 °C. Measured δ¹⁸O for gold-bearing quartz (+11.5 to +16.0‰), δD from FI (−50.6 to −21.8‰), δ¹³C from FI (−5.8 to −5.5‰), and δ³⁴S from galena and pyrite grains (+5.3‰ and +8.2‰, respectively) suggest a metamorphic source as most likely for the ore-forming fluids and sulfur, although a mantelic CO2 contribution cannot be ruled out. The gold deposition probably took place by fluid-rock interaction and fluid unmixing at ∼310 °C and at a depth of about 6-9 km. The ore-forming fluid was a low salinity (∼6.2 wt% NaCl eq.) H2O-NaCl-CO2±N2±CH4 solution. These data revealed that the Lom Belt gold mineralization is best classified as a mesozonal orogenic gold deposit.
... The PC2-FIL and PC3-FIL anomaly B coincides with the mineralized veins NW of the maps (Fig. 12b, c). This anomaly highlights two potential phases of mineralization: The first being linked to PC3-FIL with the Au-Rb-As association representing a mineralization linked to the placement of granitoids as shown by (Asaah et al. 2015;Ateh et al. 2017). These authors associate the placement of granitoids dating from 620 to 640 Ma with gold mineralization in the Batouri gold district (to the south of the study area) and Betare Oya gold district (located to the north-west part of the study area), respectively. ...
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Gold enrichment and other metals usually occur during fractional crystallization in granitoids. In this study, the spatial analysis of multi-element associations from stream sediments is proposed to identify the characteristics and distributions of lithological units and mineralized pegmatite vein with associated stream sediments in the Lingbim-Zimbi gold field for mineral exploration purposes. The sampling campaign was carried out both on rocks and in exploration wells. Principal component analysis and the phased array approach have allowed distinguishing the chemical elements linked to the mineralized structure from those linked to the geology of the area. Then, two potential gold mineralization phases were identified along with the anomalies observed and the spatial distribution of the elemental associations; the first one being linked to the emplacement of granitoids and the second linked to the formation of the Central Cameroonian Shear Zone (CCSZ) oriented NE-SW